CAS号：

593-71-5

3D弹球模型：

立即前往扯扯看

分子式：

ClCH2I

分子量：

176.3841

中文名称：

氯碘甲烷

英文名称：

Chloroiodomethane

中文别名：

氯碘甲烷;
氯碘代甲烷;
1-氯-1-碘甲烷;
MHH;
O-Methylhydroxyamine Hydrochloride;
O-Methylhydroxylamine Hcl;
O-Methylhydroxylamine Hydrochloride;
O-Methylhydroxylammonium Chloride;
Mox Reagent;
Mox(Tm) Reagent;
Hydroxylamine Methyl Ether Hydrochloride;
Mah;
(Aminooxy)Methane Hydrochloride (1:1);
Methoxyamine Hydrochloride;
methoxylamine hydrochloride;
UN1646;
Mercury(II) thiocyanate;
zoba eg;
M-Aminophenol;
m-amino phenol;
Meta Aminophenol;
Aminophenol, 3-;
3-Aminophenol;
Antigene MB;
Zinc salt of 2-mercaptobenzimidazol;
1-sulfanyl-1H-benzimidazole;
1H-benzimidazole-2-thiol;
2-meracapto-benzimidazole;
Rubber Antioxidant MB;
Antioxidant MBI;
Antioxidant MB(MBI);
2-Mercaptobenzimidazole;
Gentiaverm;
Hectograph violet;
hectograph violet sr;
hecto violet r;
hexamethylparaosaniline chloride;
hexamethyl-p-rosaniline chloride;
hexamethyl-p-rosaniline hydrochloride;
Hexamethyl Violet;
hidaco crystal violet;
Meroxyl;
Meroxylan;
meroxylanwander;
Methanaminium, N-[4-[bis[4-(dimethylamino)phenyl]methylene]-2,5-cyclohexadien-1-yli;
Basic Violet 3

英文别名：

Chloroiodomethane;
METHYLENE CHLOROIODIDE;
Methane, chloroiodo-;
Chloroiodomethane, STAB;
1-chloro-1-iodomethane;
O-Methylhydroxylamine Hcl;
O-Methylhydroxylamine Hydrochloride;
O-Methylhydroxylammonium Chloride;
Mox Reagent;
Mox(Tm) Reagent;
Hydroxylamine Methyl Ether Hydrochloride;
Mah;
(Aminooxy)Methane Hydrochloride (1:1);
Methoxyamine Hydrochloride;
methoxylamine hydrochloride;
UN1646;
Mercury(II) thiocyanate;
zoba eg;
M-Aminophenol;
m-amino phenol;
Meta Aminophenol;
Aminophenol, 3-;
3-Aminophenol;
Antigene MB;
Zinc salt of 2-mercaptobenzimidazol;
1-sulfanyl-1H-benzimidazole;
1H-benzimidazole-2-thiol;
2-meracapto-benzimidazole;
Rubber Antioxidant MB;
Antioxidant MBI;
Antioxidant MB(MBI);
2-Mercaptobenzimidazole;
Gentiaverm;
Hectograph violet;
hectograph violet sr;
hecto violet r;
hexamethylparaosaniline chloride;
hexamethyl-p-rosaniline chloride;
hexamethyl-p-rosaniline hydrochloride;
Hexamethyl Violet;
hidaco crystal violet;
Meroxyl;
Meroxylan;
meroxylanwander;
Methanaminium, N-[4-[bis[4-(dimethylamino)phenyl]methylene]-2,5-cyclohexadien-1-yli;
Ba

贝尔斯坦号/MDL：

MFCD00001078

EINECS：

209-804-8

PubChem：

24854979

BRN：

1730802

InChI：

InChI=1/CH2ClI/c2-1-3/h1H2

合成制备方法

1、生产方法简介

将二氯甲烷与碘化钠混合，在室温下搅拌，滴加二甲基甲酰胺。加毕，升温至反应物缓缓回流（约71℃）10h。静置过夜后进行水蒸气蒸馏，从馏出液中分出有机层，用水洗涤，有机层干燥后分馏得到氯碘甲烷。

2.在装有磁力搅拌器、顶端有干燥管的回流冷凝器、温度计和滴液漏斗的100毫升.--._,颈烧瓶中，放置120克(8.0摩尔)碘化钠和320克(3.76摩尔)二氯甲烷，在室温搅拌下，于5分钟内滴加240毫升二甲基甲酞胺。徐徐加热，使缓缓回流(约71℃)10小时，然后静置过夜。水蒸气蒸馏，分出有机层，用水洗涤。水层用二抓甲烷萃取，萃取液经水洗涤后合并于有机层中，加氯化钙干燥。经松针分馏柱分馏得93.5克产品(按碘化钠计，产率63%)，